Urea perchlorate
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The compound is synthesized by gradual addition of urea into a perchloric acid solution:
- CO(NH2)2 + HClO4 → CO(NH2)2·HClO4
An alternative route is addition of urea to hydrochloric acid solution, followed by addition of sodium perchlorate, and filtration of the salt.
- NaClO4·H2O + CO(NH2)2 + HCl → CO(NH2)2·HClO4 + NaCl + H2O

